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Lab 8 - Synthesis of (E) and (Z)-1-(4-bromophenyl)-2-phenylethene
https://www.youtube.com/watch?v=-e5gL3tHr48&feature=youtu.be-- Lab Manual chapter with writing assignment, background, and experimental details for Lab 8
-- The 1H-NMR (taken on a 500 MHz) doc attached includes NMRs of the crude (contains both E and Z) and recrystallized (only E).
-- The IR Spectrum attached is of the E product (this doc also has a 400 MHz NMR of the product I made this week, but this NMR is not as well-resolved so I recommend using the one taken on the 500 MHz).
-- Lab notebook pages Grading Rubric used in Spring 2020
-- JChemEd Article it is based on
-- Rubric for Lab 8 writing assignment
Lab 9 - Reductive Amination: Synthesis of N-(2-hydroxy-3-methoxybenzyl)-N-p-tolylacetamide
https://youtu.be/CpIFY_ECyCo -- Lab Manual chapter with writing assignment, background, and experimental details for Lab 9
-- Amide 1H-NMR (taken on a 500 MHz, w my loose assignment notes) + Amide IR
-- Imine 1H-NMR (not recrystallized -- messy! including in case you want your students to assign starting material peaks) and Imine IR
-- Lab notebook pages Grading Rubric used in Spring 2020
-- JChemEd Article it is based on
-- Rubric for Lab 9 writing assignment
Lab 10 - Synthesis and Chemiluminescence of Bis[2-(methoxycarbonyl)phenyl] Oxalate
https://youtu.be/cxyE-11_iuE -- Lab Manual chapter with writing assignment, background, and experimental details for Lab 10
-- 1H-NMR (taken on a 400 MHz NMR)
-- Lab notebook pages Grading Rubric used in Spring 2020
-- Rubric for Lab 10 writing assignment